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These samples were stored overnight at ambient temperature and then desorbed with 1 mL of a 1:1 solution of deionized water:methanol for 30 minutes on the shaker. A 0.5 mL aliquot of each sample was removed and added to 0.5 mL of a 1:4 solution of 1.0 N NaOH:methanol and analyzed by GC-FID.

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